Araştırma Makalesi
BibTex RIS Kaynak Göster

Yıl 2023, Cilt: 7 Sayı: 1, 131 - 135, 27.03.2023

Tarık Balkan Kenan Kara

https://doi.org/10.31015/jaefs.2023.1.16

Öz

Anahtar Kelimeler

Pesticide residue Processing factor Sauce Tomato LC-MS/MS Pesticide residue Processing factor Sauce Tomato LC-MS/MS QuEChERS

Kaynakça

  • Acoğlu, B., Yolcı Ömeroğlu, P., & Çopur, Ö.U. (2018). Gıda İşleme Süreçlerinin Pestisit Kalıntıları Üzerine Etkisi ve İşleme Faktörleri. Gıda ve Yem Bilimi Teknolojisi Dergisi, 19, 42-54. Retrieved from: https://dergipark.org.tr/tr/pub/bursagida/issue/40169/477821
  • Bakırcı G.T., Acay D.B.Y., Bakırcı F., & Ötleş S. (2014). Pesticide residues in fruits and vegetables from the Aegean region, Turkey. Food Chemistry, 160, 379-392. Doi: https://doi.org/10.1016/j.foodchem.2014.02.051
  • Balkan, T., Kara, K. (2019). Tokat İlinde Tüketime Sunulan Domateslerde Neonikotinoid Grubu İnsektisitlerin Kalıntı Düzeylerinin Belirlenmesi Üzerine Araştırmalar Gaziosmanpaşa Bilimsel Araştırma Dergisi (Gbad), 8 (3), 50-58. Retrieved from: https://dergipark.org.tr/tr/pub/gbad/issue/50458/643592
  • Balkan, T., Kara, K. (2022). Determination of Pesticide Residues and Risk Assessment in Some Vegetables Grown in Tokat Province, Plant Protection Bulletin, 62 (2), 26-35. Doi: https://doi.org/10.16955/bitkorb.1053952
  • Balkan, T., Karaağaçlı, H. (2022). Determination of 301 pesticide residues in tropical fruits imported to Turkey using LC–MS/MS and GC-MS. Food Control, 109576. Doi: https://doi.org/10.1016/j.foodcont.2022.109576
  • Balkan, T., Yılmaz, Ö. (2022). Method validation, residue and risk assessment of 260 pesticides in some leafy vegetables using liquid chromatography coupled to tandem mass spectrometry. Food Chemistry, 384:132516. Doi: https://doi.org/10.1016/j.foodchem.2022.132516
  • Burchat, C.S., Ripley, B.D., Leishman, P.D., Ritcey, G.M., Kakuda, Y., Stephenson, G.R. (1998). The distribution of nine pesticides between the juice and pulp of carrots and tomatoes after home processing. Food Addit Contam 15, 61–71. Doi: https://doi.org/10.1080/02652039809374599
  • Cengiz, M.F., Certel, M., Karakas, B., Gocmen, H. (2007). Residue contents of captan and procymidone applied on tomatoes grown in greenhouses and their reduction by duration of a pre-harvest interval and post-harvest culinary applications. Food Chemistry, 100, 1611-1619. Doi: https://doi.org/10.1016/j.foodchem.2005.12.059
  • Dülger, H., Tiryaki, O. (2022). Verification of an effective method for some pesticide residues determination in nectarine and peach samples. COMU Journal of Agriculture Faculty, 10 (1), 69-75. Doi: https://doi.org/10.33202comuagri.1006612
  • EC, 2022. European Commission, European Union (EU) pesticides database. Pesticide Residues MRLs. Directorate General for Health & Consumers. Retrieved from: https://ec.europa.eu/food/plant/pesticides/eu-pesticides-database/start/screen/mrls Accessed date: 29.10.2022
  • EFSA, European Food Safety Authority. (2018). The 2016 European Union report on pesticides residues in food. EFSA Journal, 16 (7), 5348. Retrieved from: https://efsa.onlinelibrary.wiley.com/doi/10.2903/j.efsa.2018.5348 Accessed date: 28.10.2022
  • EPA, U.S. Environmental Protection Agency. (2022). What is Pesticide? Retrieved from: https://www.epa.gov/minimum-risk-pesticides/what-pesticide Accessed date: 28.10.2022
  • Ersoy, N., Tatlı Ö., Özcan S., Evcil E., Coşkun L.Ş., Erdoğan E. (2011). Determination of pesticide residues in some vegetable species by LC-MS/MS and GC-MS. Selçuk Tarım ve Gıda Bilimleri Dergisi, 25 (3), 79-85.
  • Frank, R., Braun, H.E., Ripley, B.D., Pitblado R. (1991). Residues of Nine Insecticides and Two Fungicides in Raw and Processed Tomatoes. Journal of Food Protection, 54 (1), 41–46. Doi: https://doi.org/10.4315/0362-028X-54.1.41
  • Fukui, N., Takatori, S., Kitagawa, Y., Okihashi, M., Kajimura, K., Obana, H. (2013). Study of multi-residue method for determining pesticide residues in processed foods manufactured from agricultural products by LC-MS/MS. Journal of the Food Hygienic Society of Japan, 54 (6), 426–433. Doi: https://doi.org/10.3358/shokueishi.54.426
  • Golge O., Kabak B. (2015). Evaluation of QuEChERS sample preparation and liquid chromatography-triple-quadrupole mass spectrometry method for the determination of 109 pesticide residues in tomatoes. Food Chemistry, 176, 319- 332. Doi: https://doi.org/10.1016/j.foodchem.2014.12.083
  • Görmez, E. (2019). Ekonomik öneme sahip endüstriyel gıdalardan üzüm, domates ve biberde kullanılan pestisitlerin gıda prosesleri sonrasi kalıntı miktarlarının karşılaştırılması, Muğla Sıtkı Koçman Üniversitesi, Aydın. 187. Retrieved from: https://tez.yok.gov.tr/UlusalTezMerkezi/TezGoster?key=wf-FPgY-5qjHEzEoOgvMs1gL3DXTR-viweMHmGMV8-LpV3Ko86q20QnZNY8wgeTO
  • Karaboğa, Ö. (2021). Şefin imzası, lezzetin tamamlayıcısı: SOSLAR. Gastronomi Dergisi. Retrieved from: https://www.gastronomidergisi.com/gida/sefin-imzasi-lezzetin-tamamlayicisi-soslar
  • Kaushik, G., Satya, S., Naik, S.N. (2009). Food processing a tool to pesticide residue dissipation – A review. Food Research International, 42 (1), 26-40, https://doi.org/10.1016/j.foodres.2008.09.009.
  • Kong, Z., Dong, F., Xu, J., Liu, X., Zhang, C., Li, J., Li, Y., Chen, X., Shan, W., Zheng, Y., (2012). Determination of difenoconazole residue in tomato during home canning by UPLC-MS/MS. Food Control 23, 542-546. Doi: https://doi.org/10.1016/j.foodcont.2011.08.028
  • Lehotay S.J. (2007). Determination of pesticide residues in foods by acetonitrile extraction and partitioning with magnesium sulfate: Collaborative Study. Journal of AOAC International, 90 (2), 485–520.
  • Polat B., Tiryaki O. (2018). Investigation of pesticide residues in tomato growing open-fields of Çanakkale province by QuEChERS method. COMU Journal of Agriculture Faculty, 6 (1), 71–79.
  • Polat B., Tiryaki O. (2019). Determination of some pesticide residues in conventional-grown and IPM-grown tomato by using QuEChERS method. Journal of Environmental Science and Health, Part B, 54 (2), 112-117. Doi: https://doi.org/10.1080/03601234.2018.1531663
  • Reddy, B.K.K., Bhuvaneswari, K., Geetha, P., Thamilarasi, N., Suganthi, A., Paramasivam. M. (2022). Effect of decontamination and processing on insecticide residues in grape (Muscat Hamburg). Environmental Science and Pollution Research, 29, 75790–75804. Doi: https://doi.org/10.1007/s11356-022-21165-2
  • SANTE, (2021). SANTE/11312/2021 Analytical quality control and method validation procedures for pesticide residues analysis in food and feed. 1–55. Retrieved from: https://www.accredia.it/app/uploads/2021/02/SANTE_11312_2021.pdf Accessed date: 29.09.2022
  • Scholz, R., Hermann, M., Michalski, B. (2017). Compilation of processing factors and evaluation of quality controlled data of food processing studies. Journal of Consumer Protection and Food Safety, 12, 3-14. Doi: https://doi.org/10.1007/s00003-016-1043-3
  • Song, L., Han, Y., Yang, J., Qin, Y., Zeng, W., Xu, S., Pan, C. (2019). Rapid single-step cleanup method for analyzing 47 pesticide residues in pepper, chili peppers and its sauce product by high performance liquid and gas chromatography-tandem mass spectrometry. Food chemistry, 279, 237–245. Doi: https://doi.org/10.1016/j.foodchem.2018.12.017
  • Soydan, K.D., Turgut, N., Yalçın, M., Turgut, C, Karakuş, P.B.K. (2021). Evaluation of pesticide residues in fruits and vegetables from the Aegean region of Turkey and assessment of risk to consumers. Environmental Science and Pollution Research, 28, 27511–27519. Doi: https://doi.org/10.1007/s11356-021-12580-y
  • Valera-Tarifa, N. M., Santiago-Valverde, R., Hernández-Torres, E., Martínez-Vidal, J. L., Garrido-Frenich, A. (2020). Development and full validation of a multiresidue method for the analysis of a wide range of pesticides in processed fruit by UHPLC-MS/MS. Food chemistry, 315, 126304. Doi: https://doi.org/10.1016/j.foodchem.2020.126304
  • Zengin E., Karaca İ., (2017). Determination of pesticide residues in tomatoes grown in greenhouse in Uşak province. Journal of Natural and Applied Sciences, 21 (2), 554-559. Doi: https://doi.org/10.19113/sdufbed.72243

Pesticide residues in sauce manufactured from agricultural products

Yıl 2023, Cilt: 7 Sayı: 1, 131 - 135, 27.03.2023

Tarık Balkan Kenan Kara

https://doi.org/10.31015/jaefs.2023.1.16

Öz

In this study, pesticide residues in sauce manufactured from agricultural products were examined. A simultaneous multiresidue analysis for 260 pesticides in sauce samples was performed using liquid chromatography with tandem mass spectrometry (LC-MS/MS). The QuEChERS AOAC 2007.01 (quick, easy, cheap, effective, rugged, and safe) was selected as the most suitable protocol for routine determination of pesticide residues. In line with the SANTE/11312/2021 guideline two parameters were used as identification criteria: retention time (RT) with a tolerance of ± 0.1 min in relation to the RT of the analyte in matrix-matched calibration standard and ion ratio tolerance below 30%. The RT deviation in positive samples was always < 0.1 min, and the ion ratio tolerance was < 30%. A total 4 different pesticides were detected in 20 sauce samples. No active ingredient was found in 16 samples. The residue levels were between 10 and 94 µg kg. The residues of acetamiprid, ametoctradin, imazalil sulfate, and metalaxyl-M were below the European Union Maximum Residue Limits (EU-MRLs).

Anahtar Kelimeler

Pesticide residue Processing factor Sauce Tomato LC-MS/MS QuEChERS

Kaynakça

  • Acoğlu, B., Yolcı Ömeroğlu, P., & Çopur, Ö.U. (2018). Gıda İşleme Süreçlerinin Pestisit Kalıntıları Üzerine Etkisi ve İşleme Faktörleri. Gıda ve Yem Bilimi Teknolojisi Dergisi, 19, 42-54. Retrieved from: https://dergipark.org.tr/tr/pub/bursagida/issue/40169/477821
  • Bakırcı G.T., Acay D.B.Y., Bakırcı F., & Ötleş S. (2014). Pesticide residues in fruits and vegetables from the Aegean region, Turkey. Food Chemistry, 160, 379-392. Doi: https://doi.org/10.1016/j.foodchem.2014.02.051
  • Balkan, T., Kara, K. (2019). Tokat İlinde Tüketime Sunulan Domateslerde Neonikotinoid Grubu İnsektisitlerin Kalıntı Düzeylerinin Belirlenmesi Üzerine Araştırmalar Gaziosmanpaşa Bilimsel Araştırma Dergisi (Gbad), 8 (3), 50-58. Retrieved from: https://dergipark.org.tr/tr/pub/gbad/issue/50458/643592
  • Balkan, T., Kara, K. (2022). Determination of Pesticide Residues and Risk Assessment in Some Vegetables Grown in Tokat Province, Plant Protection Bulletin, 62 (2), 26-35. Doi: https://doi.org/10.16955/bitkorb.1053952
  • Balkan, T., Karaağaçlı, H. (2022). Determination of 301 pesticide residues in tropical fruits imported to Turkey using LC–MS/MS and GC-MS. Food Control, 109576. Doi: https://doi.org/10.1016/j.foodcont.2022.109576
  • Balkan, T., Yılmaz, Ö. (2022). Method validation, residue and risk assessment of 260 pesticides in some leafy vegetables using liquid chromatography coupled to tandem mass spectrometry. Food Chemistry, 384:132516. Doi: https://doi.org/10.1016/j.foodchem.2022.132516
  • Burchat, C.S., Ripley, B.D., Leishman, P.D., Ritcey, G.M., Kakuda, Y., Stephenson, G.R. (1998). The distribution of nine pesticides between the juice and pulp of carrots and tomatoes after home processing. Food Addit Contam 15, 61–71. Doi: https://doi.org/10.1080/02652039809374599
  • Cengiz, M.F., Certel, M., Karakas, B., Gocmen, H. (2007). Residue contents of captan and procymidone applied on tomatoes grown in greenhouses and their reduction by duration of a pre-harvest interval and post-harvest culinary applications. Food Chemistry, 100, 1611-1619. Doi: https://doi.org/10.1016/j.foodchem.2005.12.059
  • Dülger, H., Tiryaki, O. (2022). Verification of an effective method for some pesticide residues determination in nectarine and peach samples. COMU Journal of Agriculture Faculty, 10 (1), 69-75. Doi: https://doi.org/10.33202comuagri.1006612
  • EC, 2022. European Commission, European Union (EU) pesticides database. Pesticide Residues MRLs. Directorate General for Health & Consumers. Retrieved from: https://ec.europa.eu/food/plant/pesticides/eu-pesticides-database/start/screen/mrls Accessed date: 29.10.2022
  • EFSA, European Food Safety Authority. (2018). The 2016 European Union report on pesticides residues in food. EFSA Journal, 16 (7), 5348. Retrieved from: https://efsa.onlinelibrary.wiley.com/doi/10.2903/j.efsa.2018.5348 Accessed date: 28.10.2022
  • EPA, U.S. Environmental Protection Agency. (2022). What is Pesticide? Retrieved from: https://www.epa.gov/minimum-risk-pesticides/what-pesticide Accessed date: 28.10.2022
  • Ersoy, N., Tatlı Ö., Özcan S., Evcil E., Coşkun L.Ş., Erdoğan E. (2011). Determination of pesticide residues in some vegetable species by LC-MS/MS and GC-MS. Selçuk Tarım ve Gıda Bilimleri Dergisi, 25 (3), 79-85.
  • Frank, R., Braun, H.E., Ripley, B.D., Pitblado R. (1991). Residues of Nine Insecticides and Two Fungicides in Raw and Processed Tomatoes. Journal of Food Protection, 54 (1), 41–46. Doi: https://doi.org/10.4315/0362-028X-54.1.41
  • Fukui, N., Takatori, S., Kitagawa, Y., Okihashi, M., Kajimura, K., Obana, H. (2013). Study of multi-residue method for determining pesticide residues in processed foods manufactured from agricultural products by LC-MS/MS. Journal of the Food Hygienic Society of Japan, 54 (6), 426–433. Doi: https://doi.org/10.3358/shokueishi.54.426
  • Golge O., Kabak B. (2015). Evaluation of QuEChERS sample preparation and liquid chromatography-triple-quadrupole mass spectrometry method for the determination of 109 pesticide residues in tomatoes. Food Chemistry, 176, 319- 332. Doi: https://doi.org/10.1016/j.foodchem.2014.12.083
  • Görmez, E. (2019). Ekonomik öneme sahip endüstriyel gıdalardan üzüm, domates ve biberde kullanılan pestisitlerin gıda prosesleri sonrasi kalıntı miktarlarının karşılaştırılması, Muğla Sıtkı Koçman Üniversitesi, Aydın. 187. Retrieved from: https://tez.yok.gov.tr/UlusalTezMerkezi/TezGoster?key=wf-FPgY-5qjHEzEoOgvMs1gL3DXTR-viweMHmGMV8-LpV3Ko86q20QnZNY8wgeTO
  • Karaboğa, Ö. (2021). Şefin imzası, lezzetin tamamlayıcısı: SOSLAR. Gastronomi Dergisi. Retrieved from: https://www.gastronomidergisi.com/gida/sefin-imzasi-lezzetin-tamamlayicisi-soslar
  • Kaushik, G., Satya, S., Naik, S.N. (2009). Food processing a tool to pesticide residue dissipation – A review. Food Research International, 42 (1), 26-40, https://doi.org/10.1016/j.foodres.2008.09.009.
  • Kong, Z., Dong, F., Xu, J., Liu, X., Zhang, C., Li, J., Li, Y., Chen, X., Shan, W., Zheng, Y., (2012). Determination of difenoconazole residue in tomato during home canning by UPLC-MS/MS. Food Control 23, 542-546. Doi: https://doi.org/10.1016/j.foodcont.2011.08.028
  • Lehotay S.J. (2007). Determination of pesticide residues in foods by acetonitrile extraction and partitioning with magnesium sulfate: Collaborative Study. Journal of AOAC International, 90 (2), 485–520.
  • Polat B., Tiryaki O. (2018). Investigation of pesticide residues in tomato growing open-fields of Çanakkale province by QuEChERS method. COMU Journal of Agriculture Faculty, 6 (1), 71–79.
  • Polat B., Tiryaki O. (2019). Determination of some pesticide residues in conventional-grown and IPM-grown tomato by using QuEChERS method. Journal of Environmental Science and Health, Part B, 54 (2), 112-117. Doi: https://doi.org/10.1080/03601234.2018.1531663
  • Reddy, B.K.K., Bhuvaneswari, K., Geetha, P., Thamilarasi, N., Suganthi, A., Paramasivam. M. (2022). Effect of decontamination and processing on insecticide residues in grape (Muscat Hamburg). Environmental Science and Pollution Research, 29, 75790–75804. Doi: https://doi.org/10.1007/s11356-022-21165-2
  • SANTE, (2021). SANTE/11312/2021 Analytical quality control and method validation procedures for pesticide residues analysis in food and feed. 1–55. Retrieved from: https://www.accredia.it/app/uploads/2021/02/SANTE_11312_2021.pdf Accessed date: 29.09.2022
  • Scholz, R., Hermann, M., Michalski, B. (2017). Compilation of processing factors and evaluation of quality controlled data of food processing studies. Journal of Consumer Protection and Food Safety, 12, 3-14. Doi: https://doi.org/10.1007/s00003-016-1043-3
  • Song, L., Han, Y., Yang, J., Qin, Y., Zeng, W., Xu, S., Pan, C. (2019). Rapid single-step cleanup method for analyzing 47 pesticide residues in pepper, chili peppers and its sauce product by high performance liquid and gas chromatography-tandem mass spectrometry. Food chemistry, 279, 237–245. Doi: https://doi.org/10.1016/j.foodchem.2018.12.017
  • Soydan, K.D., Turgut, N., Yalçın, M., Turgut, C, Karakuş, P.B.K. (2021). Evaluation of pesticide residues in fruits and vegetables from the Aegean region of Turkey and assessment of risk to consumers. Environmental Science and Pollution Research, 28, 27511–27519. Doi: https://doi.org/10.1007/s11356-021-12580-y
  • Valera-Tarifa, N. M., Santiago-Valverde, R., Hernández-Torres, E., Martínez-Vidal, J. L., Garrido-Frenich, A. (2020). Development and full validation of a multiresidue method for the analysis of a wide range of pesticides in processed fruit by UHPLC-MS/MS. Food chemistry, 315, 126304. Doi: https://doi.org/10.1016/j.foodchem.2020.126304
  • Zengin E., Karaca İ., (2017). Determination of pesticide residues in tomatoes grown in greenhouse in Uşak province. Journal of Natural and Applied Sciences, 21 (2), 554-559. Doi: https://doi.org/10.19113/sdufbed.72243
Toplam 30 adet kaynakça vardır.

Ayrıntılar

Birincil Dil İngilizce
Konular Ziraat Mühendisliği (Diğer)
Bölüm Makaleler
Yazarlar

Tarık Balkan 0000-0003-4756-4842

Kenan Kara 0000-0003-0439-5639

Yayımlanma Tarihi 27 Mart 2023
Gönderilme Tarihi 14 Kasım 2022
Kabul Tarihi 25 Aralık 2022
Yayımlandığı Sayı Yıl 2023 Cilt: 7 Sayı: 1

Kaynak Göster

APA Balkan, T., & Kara, K. (2023). Pesticide residues in sauce manufactured from agricultural products. International Journal of Agriculture Environment and Food Sciences, 7(1), 131-135. https://doi.org/10.31015/jaefs.2023.1.16
AMA Balkan T, Kara K. Pesticide residues in sauce manufactured from agricultural products. int. j. agric. environ. food sci. Mart 2023;7(1):131-135. doi:10.31015/jaefs.2023.1.16
Chicago Balkan, Tarık, ve Kenan Kara. “Pesticide Residues in Sauce Manufactured from Agricultural Products”. International Journal of Agriculture Environment and Food Sciences 7, sy. 1 (Mart 2023): 131-35. https://doi.org/10.31015/jaefs.2023.1.16.
EndNote Balkan T, Kara K (01 Mart 2023) Pesticide residues in sauce manufactured from agricultural products. International Journal of Agriculture Environment and Food Sciences 7 1 131–135.
IEEE T. Balkan ve K. Kara, “Pesticide residues in sauce manufactured from agricultural products”, int. j. agric. environ. food sci., c. 7, sy. 1, ss. 131–135, 2023, doi: 10.31015/jaefs.2023.1.16.
ISNAD Balkan, Tarık - Kara, Kenan. “Pesticide Residues in Sauce Manufactured from Agricultural Products”. International Journal of Agriculture Environment and Food Sciences 7/1 (Mart 2023), 131-135. https://doi.org/10.31015/jaefs.2023.1.16.
JAMA Balkan T, Kara K. Pesticide residues in sauce manufactured from agricultural products. int. j. agric. environ. food sci. 2023;7:131–135.
MLA Balkan, Tarık ve Kenan Kara. “Pesticide Residues in Sauce Manufactured from Agricultural Products”. International Journal of Agriculture Environment and Food Sciences, c. 7, sy. 1, 2023, ss. 131-5, doi:10.31015/jaefs.2023.1.16.
Vancouver Balkan T, Kara K. Pesticide residues in sauce manufactured from agricultural products. int. j. agric. environ. food sci. 2023;7(1):131-5.
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