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Investigation of structural properties of Pr-doped hydroxyapatites synthesized via an ultrasonic-assisted wet chemical method

Yıl 2023, Cilt: 6 Sayı: 1, 83 - 86, 21.06.2023

Tankut Ateş Niyazi Bulut Omer Kaygılı Serhat Keser

https://doi.org/10.54565/jphcfum.1287104

Öz

In this study, the effects of the duration of ultrasonication for Pr-doped hydroxyapatite (HA) were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM) and Fourier transform infrared (FT-IR) analyses. 0.25at.%Pr-containing HA samples were prepared by the ultrasonic-assisted wet chemical route using different ultrasonication times of 0, 30, 60, 90, and 120 min. The formation of the HA phase was confirmed by the FT-IR and XRD data for each sample. The morphology was significantly affected by the duration of ultrasonication. Compared to the untreated sample, remarkable decreases in both the crystallite size and the crystallinity were observed with the duration of ultrasonication.

Anahtar Kelimeler

Bioceramics X-ray techniques Hydroxyapatite

Destekleyen Kurum

Unit of Scientific Research Projects of Firat University (FUBAP)

Proje Numarası

FF.23.12 and FF.23.13

Teşekkür

This work was supported by the Management Unit of Scientific Research Projects of Firat University (FUBAP) (Project Numbers: FF.23.12 and FF.23.13).

Kaynakça

  • [1] J. P. Monte, A. Fontes, B. S. Santos, G. A. L. Pereira and G. Pereira. Recent advances in hydroxyapatite/polymer/silver nanoparticles scaffolds with antimicrobial activity for bone regeneration. Materials Letters. 2023;338:134027. doi:https://doi.org/10.1016/j.matlet.2023.134027.
  • [2] H. G. Ateş, O. Kaygili, N. Bulut, F. Osmanlıoğlu, S. Keser, B. Tatar, B. K. Mahmood, T. Ates, F. Ercan, I. Ercan, B. Ates and İ. Özcan. Investigation of the structural, thermal, magnetic and cell viability properties of Ce/Sr co-doped hydroxyapatites. Journal of Molecular Structure. 2023;1283:135318. doi:https://doi.org/10.1016/j.molstruc.2023.135318.
  • [3] P. Rouhani, N. Taghavinia and S. Rouhani. Rapid growth of hydroxyapatite nanoparticles using ultrasonic irradiation. Ultrasonics Sonochemistry. 2010;17(5):853–856. doi:https://doi.org/10.1016/j.ultsonch.2010.01.010.
  • [4] O. Kaygili and S. Keser. Sol–gel synthesis and characterization of Sr/Mg, Mg/Zn and Sr/Zn co-doped hydroxyapatites. Materials Letters. 2015;141:161–164. doi:https://doi.org/10.1016/j.matlet.2014.11.078.
  • [5] N. A. S. Mohd Pu’ad, R. H. Abdul Haq, H. Mohd Noh, H. Z. Abdullah, M. I. Idris and T. C. Lee. Synthesis method of hydroxyapatite: A review. Materials Today: Proceedings. 2020;29(1):233–239. doi:https://doi.org/10.1016/j.matpr.2020.05.536.
  • [6] T. Baskaran, N. F. Mohammad, S. S. Md Saleh, N. F. Mohd Nasir and F. D. Mohd Daud. Synthesis Methods of Doped Hydroxyapatite: A Brief Review. Journal of Physics: Conference Series. 2021;2071:012008. doi:https://doi.org/10.1088/1742-6596/2071/1/012008.
  • [7] L. Ibrahimzade, O. Kaygili, S. Dundar, T. Ates, S. V. Dorozhkin, N. Bulut, S. Koytepe, F. Ercan, C. Gürses and A. H. Hssain. Theoretical and experimental characterization of Pr/Ce co-doped hydroxyapatites. Journal of Molecular Structure. 2021;1240:130557. doi:https://doi.org/10.1016/j.molstruc.2021.130557.
  • [8] B. D. Cullity. Elements of X-ray Diffraction, Addison, Wesley Mass: 1978. p. 127–131.
  • [9] E. Landi, A. Tampieri, G. Celotti and S. Sprio. Densification behaviour and mechanisms of synthetic hydroxyapatites. Journal of the European Ceramic Society. 2000;20(14-15):2377–2387. doi:https://doi.org/10.1016/s0955-2219(00)00154-0.
  • [10] S. Kumar Balu, P. Bargavi, S. Chitra, S. Kannan, R. Ramadoss and S. Andra. Morphological evaluation of HAp nanostructures and its shape-dependent protein adsorption study. Materials Letters. 2023;331:133491. doi:https://doi.org/10.1016/j.matlet.2022.133491.
  • [11] T. Ates, S. Keser, N. Bulut and O. Kaygili. The effects of duration of ultrasonication on the morphology and structural properties of Ni-doped hydroxyapatite structure. Journal of Physical Chemistry and Functional Materials. 2022;5(2):22–25. doi:https://doi.org/10.54565/jphcfum.1193117.

Yıl 2023, Cilt: 6 Sayı: 1, 83 - 86, 21.06.2023

Tankut Ateş Niyazi Bulut Omer Kaygılı Serhat Keser

https://doi.org/10.54565/jphcfum.1287104

Öz

Proje Numarası

FF.23.12 and FF.23.13

Kaynakça

  • [1] J. P. Monte, A. Fontes, B. S. Santos, G. A. L. Pereira and G. Pereira. Recent advances in hydroxyapatite/polymer/silver nanoparticles scaffolds with antimicrobial activity for bone regeneration. Materials Letters. 2023;338:134027. doi:https://doi.org/10.1016/j.matlet.2023.134027.
  • [2] H. G. Ateş, O. Kaygili, N. Bulut, F. Osmanlıoğlu, S. Keser, B. Tatar, B. K. Mahmood, T. Ates, F. Ercan, I. Ercan, B. Ates and İ. Özcan. Investigation of the structural, thermal, magnetic and cell viability properties of Ce/Sr co-doped hydroxyapatites. Journal of Molecular Structure. 2023;1283:135318. doi:https://doi.org/10.1016/j.molstruc.2023.135318.
  • [3] P. Rouhani, N. Taghavinia and S. Rouhani. Rapid growth of hydroxyapatite nanoparticles using ultrasonic irradiation. Ultrasonics Sonochemistry. 2010;17(5):853–856. doi:https://doi.org/10.1016/j.ultsonch.2010.01.010.
  • [4] O. Kaygili and S. Keser. Sol–gel synthesis and characterization of Sr/Mg, Mg/Zn and Sr/Zn co-doped hydroxyapatites. Materials Letters. 2015;141:161–164. doi:https://doi.org/10.1016/j.matlet.2014.11.078.
  • [5] N. A. S. Mohd Pu’ad, R. H. Abdul Haq, H. Mohd Noh, H. Z. Abdullah, M. I. Idris and T. C. Lee. Synthesis method of hydroxyapatite: A review. Materials Today: Proceedings. 2020;29(1):233–239. doi:https://doi.org/10.1016/j.matpr.2020.05.536.
  • [6] T. Baskaran, N. F. Mohammad, S. S. Md Saleh, N. F. Mohd Nasir and F. D. Mohd Daud. Synthesis Methods of Doped Hydroxyapatite: A Brief Review. Journal of Physics: Conference Series. 2021;2071:012008. doi:https://doi.org/10.1088/1742-6596/2071/1/012008.
  • [7] L. Ibrahimzade, O. Kaygili, S. Dundar, T. Ates, S. V. Dorozhkin, N. Bulut, S. Koytepe, F. Ercan, C. Gürses and A. H. Hssain. Theoretical and experimental characterization of Pr/Ce co-doped hydroxyapatites. Journal of Molecular Structure. 2021;1240:130557. doi:https://doi.org/10.1016/j.molstruc.2021.130557.
  • [8] B. D. Cullity. Elements of X-ray Diffraction, Addison, Wesley Mass: 1978. p. 127–131.
  • [9] E. Landi, A. Tampieri, G. Celotti and S. Sprio. Densification behaviour and mechanisms of synthetic hydroxyapatites. Journal of the European Ceramic Society. 2000;20(14-15):2377–2387. doi:https://doi.org/10.1016/s0955-2219(00)00154-0.
  • [10] S. Kumar Balu, P. Bargavi, S. Chitra, S. Kannan, R. Ramadoss and S. Andra. Morphological evaluation of HAp nanostructures and its shape-dependent protein adsorption study. Materials Letters. 2023;331:133491. doi:https://doi.org/10.1016/j.matlet.2022.133491.
  • [11] T. Ates, S. Keser, N. Bulut and O. Kaygili. The effects of duration of ultrasonication on the morphology and structural properties of Ni-doped hydroxyapatite structure. Journal of Physical Chemistry and Functional Materials. 2022;5(2):22–25. doi:https://doi.org/10.54565/jphcfum.1193117.
Toplam 11 adet kaynakça vardır.

Ayrıntılar

Birincil Dil İngilizce
Konular Malzeme Üretim Teknolojileri
Bölüm Makaleler
Yazarlar

Tankut Ateş 0000-0002-4519-2953

Niyazi Bulut 0000-0003-2863-7700

Omer Kaygılı 0000-0002-2321-1455

Serhat Keser 0000-0002-9678-1053

Proje Numarası FF.23.12 and FF.23.13
Yayımlanma Tarihi 21 Haziran 2023
Gönderilme Tarihi 24 Nisan 2023
Kabul Tarihi 14 Haziran 2023
Yayımlandığı Sayı Yıl 2023 Cilt: 6 Sayı: 1

Kaynak Göster

APA Ateş, T., Bulut, N., Kaygılı, O., Keser, S. (2023). Investigation of structural properties of Pr-doped hydroxyapatites synthesized via an ultrasonic-assisted wet chemical method. Journal of Physical Chemistry and Functional Materials, 6(1), 83-86. https://doi.org/10.54565/jphcfum.1287104
AMA Ateş T, Bulut N, Kaygılı O, Keser S. Investigation of structural properties of Pr-doped hydroxyapatites synthesized via an ultrasonic-assisted wet chemical method. Journal of Physical Chemistry and Functional Materials. Haziran 2023;6(1):83-86. doi:10.54565/jphcfum.1287104
Chicago Ateş, Tankut, Niyazi Bulut, Omer Kaygılı, ve Serhat Keser. “Investigation of Structural Properties of Pr-Doped Hydroxyapatites Synthesized via an Ultrasonic-Assisted Wet Chemical Method”. Journal of Physical Chemistry and Functional Materials 6, sy. 1 (Haziran 2023): 83-86. https://doi.org/10.54565/jphcfum.1287104.
EndNote Ateş T, Bulut N, Kaygılı O, Keser S (01 Haziran 2023) Investigation of structural properties of Pr-doped hydroxyapatites synthesized via an ultrasonic-assisted wet chemical method. Journal of Physical Chemistry and Functional Materials 6 1 83–86.
IEEE T. Ateş, N. Bulut, O. Kaygılı, ve S. Keser, “Investigation of structural properties of Pr-doped hydroxyapatites synthesized via an ultrasonic-assisted wet chemical method”, Journal of Physical Chemistry and Functional Materials, c. 6, sy. 1, ss. 83–86, 2023, doi: 10.54565/jphcfum.1287104.
ISNAD Ateş, Tankut vd. “Investigation of Structural Properties of Pr-Doped Hydroxyapatites Synthesized via an Ultrasonic-Assisted Wet Chemical Method”. Journal of Physical Chemistry and Functional Materials 6/1 (Haziran 2023), 83-86. https://doi.org/10.54565/jphcfum.1287104.
JAMA Ateş T, Bulut N, Kaygılı O, Keser S. Investigation of structural properties of Pr-doped hydroxyapatites synthesized via an ultrasonic-assisted wet chemical method. Journal of Physical Chemistry and Functional Materials. 2023;6:83–86.
MLA Ateş, Tankut vd. “Investigation of Structural Properties of Pr-Doped Hydroxyapatites Synthesized via an Ultrasonic-Assisted Wet Chemical Method”. Journal of Physical Chemistry and Functional Materials, c. 6, sy. 1, 2023, ss. 83-86, doi:10.54565/jphcfum.1287104.
Vancouver Ateş T, Bulut N, Kaygılı O, Keser S. Investigation of structural properties of Pr-doped hydroxyapatites synthesized via an ultrasonic-assisted wet chemical method. Journal of Physical Chemistry and Functional Materials. 2023;6(1):83-6.